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Laboratori d'Energia

El Laboratori d'Energia de l'ICIQ té com a objectiu analitzar els productes derivats de la reducció de CO2. Els productes gasosos d'aquesta reacció es poden analitzar en línia o fora de línia mitjançant cromatografia de gasos. D'altra banda, els productes de la reacció en fase líquida es poden analitzar mitjançant cromatografia iònica. El laboratori també posa a disposició dels usuaris potenciostats per al seu ús en reaccions electroquímiques i el subministrament dels gasos necessaris.



Blocs de contingut

Imatges

Potentiostat 1: SP-150 from BioLogic Science Instruments

The SP–150e is the only ampere capable electrochemical workstation to boast high-current capability (800 A with boosters), three EIS quality indicators (THD, NSD, NSR) for Electrochemical Impedance Spectroscopy validation and Ethernet compatibility for improved group-working.

Potentiostat 2: Autolab Vionic from Metrohm

VIONIC powered by INTELLO combines experimental possibilities, intelligent software, and the most complete data in one setup. Highest combination of specifications in one single instrument. Electrochemical Impedance Spectroscopy (EIS) up to 10 MHz. Selectable floating allowing you to use any cell you want. Analog scan for accurately measuring processes at the interface. Second sense (S2) for obtaining additional information from the electrochemical cell

4 Mass Flow Controllers (MFC)

Alicat Scientific, model Mass Flow Controller, 0-100, SCCM with display. Gas flow products by Alicat Scientific come in mass flow controller and mass flow meter solutions. Gas flow controllers and meters provide mass — or volumetric — flow measurement, accuracy, and lightning fast control.

Ion Chromatograph 930 Compact IC Flex from Metrohm

There are two possible configurations, one to analyze anions and another one to analyze cations. The ions that can be analyzed are the following: Anions: Acetate, Oxalate, Formiate, Nitrate, Nitrite, Chloride, Bromide and Fluoride and Sulfate. The cations to analyze: Ammonium, Hydroxylamine In addition, many other ions and it’s the ideal solution for pharmaceutical testing of Active Pharmaceutical Ingredients (APIs), impurities, and excipients.

2 Gas chromatographs GC-FID-TCD

6890 Agilent eqquiped with a methanizer and 3 valves. From the gas phase: CO2, Ethene, Ethane, H2, N2, O2, Methane, CO. In addition to the analysis of other gases qualitatively and quantitatively in ppm concentrations.

Gas chromatograph Agilent 8890 GC fitted with a pulsed discharge helium ionization detector (PDHID)

An Agilent 8890 GC equipped with an off-the-shelf pulsed discharge helium ionization detector (PDHID) was used to detect ppb to low ppm concentrations of carbon dioxide, carbon monoxide, methane, argon, oxygen, nitrogen, and other impurities in high-purity hydrogen. The GC method provided low detection limits, good reproducibility, and excellent linearity.

Sampling canisters Air Sampling Canister

1 L, with 3-Port RAVE+ Valve with Gauge. Regulate the collection, storage, and analysis of volatile organic compounds (VOCs) using treated air sampling vessels. A unique bracket secures the handle and base to the vessel without welding and protects the vessel, tube end, and valve. The valve is 2/3-turn, with an exceptionally high-quality metal-to-metal seal and metal diaphragms to prevent sample adsorption and achieve more accurate results. Each vessel is lightly pressurized with contaminant-free nitrogen before

Contactes institucionals / Cap de plataformes

Dades provisionals

Dra. Gisela Colet - gcolet@iciq.cat

Tècnic

María José Hueso |   mhueso@iciq.es  | 977 920 200 (ext. 332)

Meritxell Díaz |   mdiaz@iciq.es  | 977 920 200 (ext. 332)

Dra. Gisela Colet | Coordinador/ a d'Instal·lacions |   gcolet@iciq.cat  | Telèfon: +34 977 920 238

Centres CERCA

Propietaris

Llista Centres CERCA

Equipament i Serveis

• Potenciostat 1: SP-150 de BioLogic Science Instruments. • Potenciostat 2: Autolab Vionic de Metrohm. • Dos cromatògrafs de gasos (GC) equipats amb dues columnes, tres vàlvules, un metanitzador i dos detectors (TCD i FID): Agilent model GC-FID-TCD 6890. • Quatre controladors de massa (MFC): Alicat Scientific, model Mass Flow Controller, 0-100, SCCM amb pantalla. • Cromatògraf d'ions (IC): 930 Compact IC Flex de Metrohm. • Recirculador de refrigerant: HUBER Ministat CC240 (-45ºC/200ºC).

Anàlisi de gasos en línia i fora de línia Anàlisi de compostos per cromatografia iònica Anàlisi de productes gasosos i dissolts resultants de la reducció de CO2 Anàlisi de productes de reaccions electroquímiques

Categorització

Dominis RIS3CAT

Dominis RIS3CAT

CERCA GINYS Categories

GINYS-ICIQ-011

Procediment d'accés i tarifes

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