Laboratorio de Energía

El Laboratorio de Energía del ICIQ tiene como objetivo analizar los productos derivados de la reducción de CO2. Los productos gaseosos de esta reacción se pueden analizar en línea o fuera de línea mediante cromatografía de gases. Por otra parte, los productos de la reacción en la fase líquida de la reacción pueden analizarse mediante cromatografía iónica. El laboratorio también pone a disposición de los usuarios potenciostatos para su uso en reacciones electroquímicas y el suministro de los gases necesarios.

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Imágenes

Potentiostat 1: SP-150 from BioLogic Science Instruments

The SP–150e is the only ampere capable electrochemical workstation to boast high-current capability (800 A with boosters), three EIS quality indicators (THD, NSD, NSR) for Electrochemical Impedance Spectroscopy validation and Ethernet compatibility for improved group-working.

Potentiostat 2: Autolab Vionic from Metrohm

VIONIC powered by INTELLO combines experimental possibilities, intelligent software, and the most complete data in one setup. Highest combination of specifications in one single instrument. Electrochemical Impedance Spectroscopy (EIS) up to 10 MHz. Selectable floating allowing you to use any cell you want. Analog scan for accurately measuring processes at the interface. Second sense (S2) for obtaining additional information from the electrochemical cell

4 Mass Flow Controllers (MFC)

Alicat Scientific, model Mass Flow Controller, 0-100, SCCM with display. Gas flow products by Alicat Scientific come in mass flow controller and mass flow meter solutions. Gas flow controllers and meters provide mass — or volumetric — flow measurement, accuracy, and lightning fast control.

Ion Chromatograph 930 Compact IC Flex from Metrohm

There are two possible configurations, one to analyze anions and another one to analyze cations. The ions that can be analyzed are the following: Anions: Acetate, Oxalate, Formiate, Nitrate, Nitrite, Chloride, Bromide and Fluoride and Sulfate. The cations to analyze: Ammonium, Hydroxylamine In addition, many other ions and it’s the ideal solution for pharmaceutical testing of Active Pharmaceutical Ingredients (APIs), impurities, and excipients.

2 Gas chromatographs GC-FID-TCD

6890 Agilent eqquiped with a methanizer and 3 valves. From the gas phase: CO2, Ethene, Ethane, H2, N2, O2, Methane, CO. In addition to the analysis of other gases qualitatively and quantitatively in ppm concentrations.

Gas chromatograph Agilent 8890 GC fitted with a pulsed discharge helium ionization detector (PDHID)

An Agilent 8890 GC equipped with an off-the-shelf pulsed discharge helium ionization detector (PDHID) was used to detect ppb to low ppm concentrations of carbon dioxide, carbon monoxide, methane, argon, oxygen, nitrogen, and other impurities in high-purity hydrogen. The GC method provided low detection limits, good reproducibility, and excellent linearity.

Sampling canisters Air Sampling Canister

1 L, with 3-Port RAVE+ Valve with Gauge. Regulate the collection, storage, and analysis of volatile organic compounds (VOCs) using treated air sampling vessels. A unique bracket secures the handle and base to the vessel without welding and protects the vessel, tube end, and valve. The valve is 2/3-turn, with an exceptionally high-quality metal-to-metal seal and metal diaphragms to prevent sample adsorption and achieve more accurate results. Each vessel is lightly pressurized with contaminant-free nitrogen before

Contacto principal

Contactos Institucionales / Responsable de Plataformas

Contactos temporales

Dra. Gisela Colet - gcolet@iciq.cat

Técnico

María José Hueso |   mhueso@iciq.es  | 977 920 200 (ext. 332)

Meritxell Díaz |   mdiaz@iciq.es  | 977 920 200 (ext. 332)

Dra. Gisela Colet | Coordinador de Instalaciones |   gcolet@iciq.cat  | Teléfono: +34 977 920 238

Centros CERCA

Propietarios

Lista Centros CERCA

Equipos y Servicios

Potenciostato 1: SP-150 de BioLogic Science Instruments. Potenciostato 2: Autolab Vionic de Metrohm. Dos cromatógrafos de gases (GC) equipados con dos columnas, tres válvulas, un metanizador y dos detectores (TCD y FID): Agilent, modelo GC-FID-TCD 6890. Cuatro controladores de masa (MFC): Alicat Scientific, modelo Mass Flow Controller, 0-100, SCCM con pantalla. Cromatógrafo iónico (CI): 930 Compact IC Flex de Metrohm. Recirculador de refrigerante: HUBER Ministat CC240 (-45 °C/200 °C).

Análisis de gases offline y online Análisis de compuestos por cromatografía iónica Análisis de productos gaseosos y disueltos resultantes de la reducción de CO2 Análisis de productos de reacciones electroquímicas

Categorización

Dominios RIS3CAT y otros

Dominios RIS3CAT

Categorías de CERCA GINYS

GINYS-ICIQ-011

Procedimiento de acceso y tarifas

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