
Electron diffraction
Facility
XtaLAB Synergy-ED 200 KeV


Gatan Cryo-Transfer Holder to -173 K
JEOL EM-21130
Institutional Contacts / Head of Facilities
GC
Provisional Contacts
CERCA Institutes

Tarragona, Spain
2004
Institut Català d'Investigació Química (ICIQ)
Owners
ICIQ
Videos
Equipments & Services Offered
XtaLAB Synergy-ED electron diffractometer. 200 KeV equiped with a hybrid pyxel detector HyPix-ED Gatan Cryo-Transfer Holder to -173 K JEOL EM-21130 oven up to 800 ºC (1073 K)
Structure of nanocrystals. The device comes furnished with an extremely fast detector and a wide-ranging goniometer, enabling full set data collection in a matter of minutes. Indexing. It allows the fast indexing of nanocrystals in seconds. In situ crystallization. The low temperature device enables in situ crystallization of sensitive samples. In situ crystallization from solvent. Measurements at 100 K. It can measure at temperatures of 100K enhancing the sample stability and the quality of the measurement. Sample preparation at 100K. The ED is equipped with an external cryostat for preserving instable samples. Oven for measurements up to 1000 K. For special analysis it owns an internal oven that reach temperatures up to 1000 K. Absolute configuration. Utilizing this methodology, it becomes feasible to determine the absolute configuration of compounds, even when the size of their crystals is merely in the range of hundreds of nanometers.
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